Manually Operated ASTM D1160 Specifications

Manual Control of Distillation including:

• Distillation rate adjusted with manual heat control
• Vacuum level adjusted with manual control valve
• Receiver/condenser temperatures set on bath

Operator manually records

• First drop (IBP)
• Vapor temperature, pot temperature, vacuum level and distillation rate at 5%, 10%, 20%....volume and final boiling point (FBP)

Boiling Flask/Heating Mantle

• 500 ml
• Borosilicate or quartz
• High wattage heating mantle
• Insulating top

Distillation Column

• According ASTM specifications
• Vertical viewing window for easy viewing
• Highly reflective vacuum jacket
• Adjustable vapor temperature probe

First Drop Detector

• Automatically detects and records the first drop (IBP)

Receiver/Volume Measurement

• Programmable receiver temperature

Circulating Bath

• Programmable
• 30-100°C Standard
• Optional -10 to 100 °C
• Low liquid cut off
• Over temperature cut off

Vacuum Operation

• Manually operated control valve

Vacuum Components

• 100-1 mmHg range standard (MKS)
• Optional 760-100 mmHg range (MKS)
• Optional 1-0.1 mmHg range (MKS)
• Control valve (MKS)
• Vacuum pump (Edwards)

Cold Trap

• Cooling by dry ice
• Optional automatic cooler, -60 °C
• Graduated
• Easy access
• Easy to see contents
• Easy to remove contents

Dimensions

• 91.5 cm x 94 cm x 53 cm (H x W x D)

Power (Distillation Unit Only)

• 10 amps 220 VAC